Effect of solvent type on the formation of tubular fullerene nanofibers

Yongtao Qu; Shaocen Liang; Kai Zou; Shaoxiang Li; Lumei Liu; Jian Zhao; Guangzhe Piao

doi:10.1016/j.matlet.2010.10.075

Effect of solvent type on the formation of tubular fullerene nanofibers

Yongtao Qu, Shaocen Liang, Kai Zou, Shaoxiang Li, Lumei Liu, Jian Zhao, Guangzhe Piao^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

25 Citations (Scopus)

Abstract

1D Fullerene C₆₀ nanofibers (FNFs) were prepared via liquid-liquid interfacial precipitation (LLIP) using toluene, m-xylene, pyridine and/or N-methyl-2-pyrrolidone (NMP) as solvents and isopropyl alcohol as the precipitation agent at 8 °C. C₆₀-saturated solutions were exposed to visible light to promote the growth of FNFs. When the solvents were toluene and m-xylene, it was difficult to synthesize hollow C₆₀ fullerene nanotubes (FNTs). By contrast, the hollow FNTs were easily grown in the C ₆₀-pyridine solution or C₆₀-NMP solution upon exposure to visible light. It is found that there is a critical correlation between the adducts of the solvents with C₆₀ molecules and the tubular structure of FNFs.

Original language	English
Pages (from-to)	562-564
Number of pages	3
Journal	Materials Letters
Volume	65
Issue number	3
DOIs	https://doi.org/10.1016/j.matlet.2010.10.075
Publication status	Published - 15 Feb 2011
Externally published	Yes

Keywords

Crystal growth
Fullerenes
Nanomaterials

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10.1016/j.matlet.2010.10.075

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@article{c1c71f77681543b2a09ae702eaa8ca5e,

title = "Effect of solvent type on the formation of tubular fullerene nanofibers",

abstract = "1D Fullerene C60 nanofibers (FNFs) were prepared via liquid-liquid interfacial precipitation (LLIP) using toluene, m-xylene, pyridine and/or N-methyl-2-pyrrolidone (NMP) as solvents and isopropyl alcohol as the precipitation agent at 8 °C. C60-saturated solutions were exposed to visible light to promote the growth of FNFs. When the solvents were toluene and m-xylene, it was difficult to synthesize hollow C60 fullerene nanotubes (FNTs). By contrast, the hollow FNTs were easily grown in the C 60-pyridine solution or C60-NMP solution upon exposure to visible light. It is found that there is a critical correlation between the adducts of the solvents with C60 molecules and the tubular structure of FNFs.",

keywords = "Crystal growth, Fullerenes, Nanomaterials",

author = "Yongtao Qu and Shaocen Liang and Kai Zou and Shaoxiang Li and Lumei Liu and Jian Zhao and Guangzhe Piao",

note = "Funding Information: Part of this research was financially supported by the National Natural Science Foundation of China ( 50773033 , 50872060 and 50943026 ), the Shandong Province Science Foundation ( Y2007F01 and Q2008F07 ) and the Doctoral Found of QUST .",

year = "2011",

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day = "15",

doi = "10.1016/j.matlet.2010.10.075",

language = "English",

volume = "65",

pages = "562--564",

journal = "Materials Letters",

issn = "0167-577X",

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T1 - Effect of solvent type on the formation of tubular fullerene nanofibers

AU - Qu, Yongtao

AU - Liang, Shaocen

AU - Zou, Kai

AU - Li, Shaoxiang

AU - Liu, Lumei

AU - Zhao, Jian

AU - Piao, Guangzhe

N1 - Funding Information: Part of this research was financially supported by the National Natural Science Foundation of China ( 50773033 , 50872060 and 50943026 ), the Shandong Province Science Foundation ( Y2007F01 and Q2008F07 ) and the Doctoral Found of QUST .

PY - 2011/2/15

Y1 - 2011/2/15

N2 - 1D Fullerene C60 nanofibers (FNFs) were prepared via liquid-liquid interfacial precipitation (LLIP) using toluene, m-xylene, pyridine and/or N-methyl-2-pyrrolidone (NMP) as solvents and isopropyl alcohol as the precipitation agent at 8 °C. C60-saturated solutions were exposed to visible light to promote the growth of FNFs. When the solvents were toluene and m-xylene, it was difficult to synthesize hollow C60 fullerene nanotubes (FNTs). By contrast, the hollow FNTs were easily grown in the C 60-pyridine solution or C60-NMP solution upon exposure to visible light. It is found that there is a critical correlation between the adducts of the solvents with C60 molecules and the tubular structure of FNFs.

AB - 1D Fullerene C60 nanofibers (FNFs) were prepared via liquid-liquid interfacial precipitation (LLIP) using toluene, m-xylene, pyridine and/or N-methyl-2-pyrrolidone (NMP) as solvents and isopropyl alcohol as the precipitation agent at 8 °C. C60-saturated solutions were exposed to visible light to promote the growth of FNFs. When the solvents were toluene and m-xylene, it was difficult to synthesize hollow C60 fullerene nanotubes (FNTs). By contrast, the hollow FNTs were easily grown in the C 60-pyridine solution or C60-NMP solution upon exposure to visible light. It is found that there is a critical correlation between the adducts of the solvents with C60 molecules and the tubular structure of FNFs.

KW - Crystal growth

KW - Fullerenes

KW - Nanomaterials

UR - https://www.scopus.com/pages/publications/78649343414

U2 - 10.1016/j.matlet.2010.10.075

DO - 10.1016/j.matlet.2010.10.075

M3 - Article

AN - SCOPUS:78649343414

SN - 0167-577X

VL - 65

SP - 562

EP - 564

JO - Materials Letters

JF - Materials Letters

IS - 3

ER -

Effect of solvent type on the formation of tubular fullerene nanofibers

Abstract

Keywords

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