Evaluation of a gas jet-enhanced sputtering device for atomic absorption spectrometry

Samantha J. O'Gram; John Dean; William R. Tomlinson; John Marshall

doi:10.1039/ja9920700229

Evaluation of a gas jet-enhanced sputtering device for atomic absorption spectrometry

Samantha J. O'Gram, John Dean, William R. Tomlinson, John Marshall

Applied Sciences Department

Research output: Contribution to journal › Review article › peer-review

3 Citations (Scopus)

Abstract

A gas jet-enhanced sputtering device has been utilized in glow discharge atomic absorption spectrometry for the analysis of solid steel samples. The experimental design was implemented in the evaluation of fundamental operating parameters (hollow cathode lamp current, burn current and burn pressure). Statistical techniques were used to determine the optimum conditions. Four samples types were considered: British Chemical Standard Certified Reference Materials SS 451/1-455/1 Carbon Steel Residual Series (Group A), SS 461-468 Austenitic Stainless Steels and SS 409/1 Low Alloy Steel (Group B), and 12671 H Cobalt-based Alloy. Sensitivities for nickel, chromium and copper determined in the carbon steel under optimum conditions were 54, 6 and 64 μg g ^-1, respectively.

Original language	English
Pages (from-to)	229-234
Number of pages	6
Journal	Journal of Analytical Atomic Spectrometry
Volume	7
Issue number	2
DOIs	https://doi.org/10.1039/ja9920700229
Publication status	Published - 1 Jan 1992

Keywords

Atomic absorption spectrometry
Experimental design
Glow discharge
Solid steel analysis

Access to Document

10.1039/ja9920700229

Cite this

@article{beaf2991067f451f81e9772e3bb559ea,

title = "Evaluation of a gas jet-enhanced sputtering device for atomic absorption spectrometry",

abstract = "A gas jet-enhanced sputtering device has been utilized in glow discharge atomic absorption spectrometry for the analysis of solid steel samples. The experimental design was implemented in the evaluation of fundamental operating parameters (hollow cathode lamp current, burn current and burn pressure). Statistical techniques were used to determine the optimum conditions. Four samples types were considered: British Chemical Standard Certified Reference Materials SS 451/1-455/1 Carbon Steel Residual Series (Group A), SS 461-468 Austenitic Stainless Steels and SS 409/1 Low Alloy Steel (Group B), and 12671 H Cobalt-based Alloy. Sensitivities for nickel, chromium and copper determined in the carbon steel under optimum conditions were 54, 6 and 64 μg g -1, respectively.",

keywords = "Atomic absorption spectrometry, Experimental design, Glow discharge, Solid steel analysis",

author = "O'Gram, {Samantha J.} and John Dean and Tomlinson, {William R.} and John Marshall",

year = "1992",

month = jan,

day = "1",

doi = "10.1039/ja9920700229",

language = "English",

volume = "7",

pages = "229--234",

journal = "Journal of Analytical Atomic Spectrometry",

issn = "0267-9477",

publisher = "Royal Society of Chemistry",

number = "2",

}

TY - JOUR

T1 - Evaluation of a gas jet-enhanced sputtering device for atomic absorption spectrometry

AU - O'Gram, Samantha J.

AU - Dean, John

AU - Tomlinson, William R.

AU - Marshall, John

PY - 1992/1/1

Y1 - 1992/1/1

N2 - A gas jet-enhanced sputtering device has been utilized in glow discharge atomic absorption spectrometry for the analysis of solid steel samples. The experimental design was implemented in the evaluation of fundamental operating parameters (hollow cathode lamp current, burn current and burn pressure). Statistical techniques were used to determine the optimum conditions. Four samples types were considered: British Chemical Standard Certified Reference Materials SS 451/1-455/1 Carbon Steel Residual Series (Group A), SS 461-468 Austenitic Stainless Steels and SS 409/1 Low Alloy Steel (Group B), and 12671 H Cobalt-based Alloy. Sensitivities for nickel, chromium and copper determined in the carbon steel under optimum conditions were 54, 6 and 64 μg g -1, respectively.

AB - A gas jet-enhanced sputtering device has been utilized in glow discharge atomic absorption spectrometry for the analysis of solid steel samples. The experimental design was implemented in the evaluation of fundamental operating parameters (hollow cathode lamp current, burn current and burn pressure). Statistical techniques were used to determine the optimum conditions. Four samples types were considered: British Chemical Standard Certified Reference Materials SS 451/1-455/1 Carbon Steel Residual Series (Group A), SS 461-468 Austenitic Stainless Steels and SS 409/1 Low Alloy Steel (Group B), and 12671 H Cobalt-based Alloy. Sensitivities for nickel, chromium and copper determined in the carbon steel under optimum conditions were 54, 6 and 64 μg g -1, respectively.

KW - Atomic absorption spectrometry

KW - Experimental design

KW - Glow discharge

KW - Solid steel analysis

UR - http://www.scopus.com/inward/record.url?scp=37049072408&partnerID=8YFLogxK

U2 - 10.1039/ja9920700229

DO - 10.1039/ja9920700229

M3 - Review article

AN - SCOPUS:37049072408

SN - 0267-9477

VL - 7

SP - 229

EP - 234

JO - Journal of Analytical Atomic Spectrometry

JF - Journal of Analytical Atomic Spectrometry

IS - 2

ER -

Evaluation of a gas jet-enhanced sputtering device for atomic absorption spectrometry

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this