Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil

Lisa Fitzpatrick; John Dean; Michael Comber; Kevin Harradine; Ken Evans

doi:10.1016/S0021-9673(00)00101-1

Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil

Lisa Fitzpatrick, John Dean, Michael Comber, Kevin Harradine, Ken Evans

Applied Sciences Department

Research output: Contribution to journal › Article › peer-review

14 Citations (Scopus)

Abstract

Pressurised liquid extraction (PLE) was used to extract DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites, DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane] and DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] from an aged, contaminated soil. Using three sequential static phases, PLE removed an equivalent quantity of DDT and its metabolites as Soxhlet extraction, in less time and with less solvent. Recovery was almost quantitative, implying appropriate sample work-up and manipulation.

Original language	English
Pages (from-to)	257-264
Journal	Journal of Chromatography A
Volume	874
Issue number	2
DOIs	https://doi.org/10.1016/S0021-9673(00)00101-1
Publication status	Published - Apr 2000

Keywords

Soil
extraction methods
pressurised liquid extraction
environmental analysis

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10.1016/S0021-9673(00)00101-1

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Fitzpatrick, L., Dean, J., Comber, M., Harradine, K., & Evans, K. (2000). Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil. Journal of Chromatography A, 874(2), 257-264. https://doi.org/10.1016/S0021-9673(00)00101-1

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title = "Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil",

abstract = "Pressurised liquid extraction (PLE) was used to extract DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites, DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane] and DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] from an aged, contaminated soil. Using three sequential static phases, PLE removed an equivalent quantity of DDT and its metabolites as Soxhlet extraction, in less time and with less solvent. Recovery was almost quantitative, implying appropriate sample work-up and manipulation.",

keywords = "Soil, extraction methods, pressurised liquid extraction, environmental analysis",

author = "Lisa Fitzpatrick and John Dean and Michael Comber and Kevin Harradine and Ken Evans",

year = "2000",

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doi = "10.1016/S0021-9673(00)00101-1",

language = "English",

volume = "874",

pages = "257--264",

journal = "Journal of Chromatography A",

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Fitzpatrick, L, Dean, J, Comber, M, Harradine, K & Evans, K 2000, 'Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil', Journal of Chromatography A, vol. 874, no. 2, pp. 257-264. https://doi.org/10.1016/S0021-9673(00)00101-1

Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil. / Fitzpatrick, Lisa; Dean, John; Comber, Michael et al.
In: Journal of Chromatography A, Vol. 874, No. 2, 04.2000, p. 257-264.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Extraction of DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] and DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane]) from aged contaminated soil

AU - Fitzpatrick, Lisa

AU - Dean, John

AU - Comber, Michael

AU - Harradine, Kevin

AU - Evans, Ken

PY - 2000/4

Y1 - 2000/4

N2 - Pressurised liquid extraction (PLE) was used to extract DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites, DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane] and DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] from an aged, contaminated soil. Using three sequential static phases, PLE removed an equivalent quantity of DDT and its metabolites as Soxhlet extraction, in less time and with less solvent. Recovery was almost quantitative, implying appropriate sample work-up and manipulation.

AB - Pressurised liquid extraction (PLE) was used to extract DDT [1,1,1,-trichloro-2,2-bis(p-chlorophenyl)ethane] and its metabolites, DDD [1,1-dichloro-2,2-bis(p-chlorophenyl)ethane] and DDE [1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene] from an aged, contaminated soil. Using three sequential static phases, PLE removed an equivalent quantity of DDT and its metabolites as Soxhlet extraction, in less time and with less solvent. Recovery was almost quantitative, implying appropriate sample work-up and manipulation.

KW - Soil

KW - extraction methods

KW - pressurised liquid extraction

KW - environmental analysis

U2 - 10.1016/S0021-9673(00)00101-1

DO - 10.1016/S0021-9673(00)00101-1

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SN - 0021-9673

VL - 874

SP - 257

EP - 264

JO - Journal of Chromatography A

JF - Journal of Chromatography A

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