Macrocyclic ethers by free radical cyclizations

Annie Philippon, Jingchao Tao, David Tétard, Marie Degueil-Castaing, Bernard Maillard*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

10 Citations (Scopus)

Abstract

Tin hydride reduction of ω-iodo-polyoxaalkyl acrylates 1 using syringe pump addition of both reactants to a solution of AIBN in benzene at 80°C afforded the corresponding cyclic polyethers in excellent yields.

Original languageEnglish
Pages (from-to)2651-2682
Number of pages32
JournalSynthetic Communications
Volume27
Issue number15
DOIs
Publication statusPublished - 1997
Externally publishedYes

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