Abstract
Tin hydride reduction of ω-iodo-polyoxaalkyl acrylates 1 using syringe pump addition of both reactants to a solution of AIBN in benzene at 80°C afforded the corresponding cyclic polyethers in excellent yields.
Original language | English |
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Pages (from-to) | 2651-2682 |
Number of pages | 32 |
Journal | Synthetic Communications |
Volume | 27 |
Issue number | 15 |
DOIs | |
Publication status | Published - 1997 |
Externally published | Yes |