Synthesis of 2,2′-bipyridyl derivatives using aza Diels-Alder methodology

Stephen Stanforth; Brian Tarbit; Michael Watson

doi:10.1016/S0040-4039(02)02670-9

Synthesis of 2,2′-bipyridyl derivatives using aza Diels-Alder methodology

Stephen Stanforth, Brian Tarbit, Michael Watson

Research output: Contribution to journal › Article › peer-review

30 Citations (Scopus)

Abstract

Amidrazone 1 and the tricarbonyl derivatives 2a-c gave the triazines 3a-c, respectively, which reacted with 2,5-norbornadiene 4 in boiling ethanol yielding the corresponding novel 2,2′-bipyridines 5a-c in good yield. Triazine 6 gave the 2,2′-bipyridyl derivative 7 (65%) with compound 4 in 1,2-dichlorobenzene at 140°C. © 2003 Elsevier Science Ltd. All rights reserved.

Original language	English
Pages (from-to)	693-694
Journal	Tetrahedron Letters
Volume	44
Issue number	4
DOIs	https://doi.org/10.1016/S0040-4039(02)02670-9
Publication status	Published - Jan 2003

Keywords

1
2
4-triazines
2′-bipyridyls
Aza Diels-Alder reaction

Access to Document

10.1016/S0040-4039(02)02670-9

Cite this

@article{ef5f4b38a7474cb68ba9c663af5789a4,

title = "Synthesis of 2,2′-bipyridyl derivatives using aza Diels-Alder methodology",

abstract = "Amidrazone 1 and the tricarbonyl derivatives 2a-c gave the triazines 3a-c, respectively, which reacted with 2,5-norbornadiene 4 in boiling ethanol yielding the corresponding novel 2,2′-bipyridines 5a-c in good yield. Triazine 6 gave the 2,2′-bipyridyl derivative 7 (65\%) with compound 4 in 1,2-dichlorobenzene at 140°C. {\textcopyright} 2003 Elsevier Science Ltd. All rights reserved.",

keywords = "1, 2, 4-triazines, 2′-bipyridyls, Aza Diels-Alder reaction",

author = "Stephen Stanforth and Brian Tarbit and Michael Watson",

year = "2003",

month = jan,

doi = "10.1016/S0040-4039(02)02670-9",

language = "English",

volume = "44",

pages = "693--694",

journal = "Tetrahedron Letters",

issn = "0040-4039",

publisher = "Elsevier",

number = "4",

}

TY - JOUR

T1 - Synthesis of 2,2′-bipyridyl derivatives using aza Diels-Alder methodology

AU - Stanforth, Stephen

AU - Tarbit, Brian

AU - Watson, Michael

PY - 2003/1

Y1 - 2003/1

N2 - Amidrazone 1 and the tricarbonyl derivatives 2a-c gave the triazines 3a-c, respectively, which reacted with 2,5-norbornadiene 4 in boiling ethanol yielding the corresponding novel 2,2′-bipyridines 5a-c in good yield. Triazine 6 gave the 2,2′-bipyridyl derivative 7 (65%) with compound 4 in 1,2-dichlorobenzene at 140°C. © 2003 Elsevier Science Ltd. All rights reserved.

AB - Amidrazone 1 and the tricarbonyl derivatives 2a-c gave the triazines 3a-c, respectively, which reacted with 2,5-norbornadiene 4 in boiling ethanol yielding the corresponding novel 2,2′-bipyridines 5a-c in good yield. Triazine 6 gave the 2,2′-bipyridyl derivative 7 (65%) with compound 4 in 1,2-dichlorobenzene at 140°C. © 2003 Elsevier Science Ltd. All rights reserved.

KW - 1

KW - 2

KW - 4-triazines

KW - 2′-bipyridyls

KW - Aza Diels-Alder reaction

UR - https://www.scopus.com/pages/publications/0037455043

U2 - 10.1016/S0040-4039(02)02670-9

DO - 10.1016/S0040-4039(02)02670-9

M3 - Article

SN - 0040-4039

VL - 44

SP - 693

EP - 694

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 4

ER -

Synthesis of 2,2′-bipyridyl derivatives using aza Diels-Alder methodology

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this